Insecticide composition

专利摘要:
N-benzoyl N'-pyridyloxy phenyl ureas having the formula <IMAGE> (I) wherein X represents a halogen atom; R represents a C1-C4 alkyl group and n is 0, 1 or 2 are useful as insecticides.
公开号:SU1322968A3
申请号:SU802977036
申请日:1980-09-05
公开日:1987-07-07
发明作者:Нисияма Риузо；Хага Такахиро；Токи Тадааки；Коянаги Тору；Мураи Сигео
申请人:Исихара Сангио Кайся Лтд (Фирма)；
IPC主号:

专利说明:

11322968
The invention relates to chemical. Kim plant protection products, conggi do
retina to the insecticidal composition in the form of a dispersion based on N-benzoyl-N-pyridyloxyphenylurea,
The purpose of the invention is the enhancement of insecticidal activity.
The invention is illustrated by examples in which the compounds shown in Table 1 are used as derivatives of H-benzoyl-K-pyridyloxyphenylurea.
I
Example 1. When conducting a biological experiment using composition 1 of the following composition, wt.%:
Derived N-benzoyl-N-pyridyloxy-
phenylureas30
Polyoxyethylene styrylphenyl
ether10
Polyox sulfate
ethylene alkylaryl ether 1 O
Water5 Oh
The above composition 1 is dispersed in water to prepare dispersions containing the corresponding active ingredients at a concentration of 400 parts. Rta 1 million. Cabbage leaves are immersed in such dispersions for 10 s after which they are removed and dried in air.
Each piece of Petri dish (9 cm in diameter) is placed on a piece of moistened filter paper, and then dried cabbage leaves are placed on these filter paper pieces, then the leaves are planted with a mint of cabbage in the second or third age stage, the lids of Petri dishes are closed and These cups are kept under constant temperature (28 C) and light conditions. After 8 days after treatment with the dispersion, the number of dead larva i is determined, and the mortality rate of the experimental animals is calculated using this equation.
Mortality rate
Number of dead larvae Total number of larvae
The results of the insecticidal compositions are given in table.
X
Example 2. Biological testing of composition 2 of the following composition, wt.%:
Derived N-benzoyl-N-pyridyloxy-phenylurea50
Polyoxyethylene alkylaryl
ether3.5
Sulfonate polyethylene alkyl-aryl ester sulfonate 1.0 Dialkylsulfonic acid 0.3
Water .45
According to example 1, these tests are carried out, but the concentrations of each active component in composition 2 are changed. The results are shown in Table 4.
Example 3: According to Example I, the larvae of the cabbage moth and tobacco moth in the second and third age stages were tested in which compositions based on known compounds were used as objects of comparison:
-so-in-sooch Vg
S1H

In O-so-kncha-T4N-o-OOCHI-C1
H Hi
T
in O-CO-NH-CO-lSlH V-O-XO CFj
FCl
The results of the insecticidal action of the compositions are given in Table 5.

权利要求:
Claims (1)
[1]
Invention Formula
An insecticidal composition in the form of an ejection based on an N-benzoyl-N-pyridyloxyphenylurea derivative, a surfactant and a solvent, characterized in that, in order to enhance the insecticidal activity, the contains a compound of formula
55
O X. X, X, C-NfrQ-O-O-CFj Xs X
313229684
where X, is hydrogen, chlorine, fluorine, bromine, arusha ether, sulfate or sulfonate
. methyl, nitro; polyoxyethylene alkylaryl ether, and
Xj is hydrogen, chlorine, fluorine; also dialkyl sulfosuccinate, the solvent is water with the following content: X — hydrogen, respectively, and 5 components, wt%,%;
Teal, chlorine {
Xj is hydrogen, chlorine, C, -C, -alkyl, methylcarbonyl, carX, and
bonil; X - methyl, nitro, labels - fO
6
hydrogen, chlorine; X - hydrogen, chlorine, fluorine, and 6poMJ, in the case when X and Xg are simultaneously a derivative of N-benzo-ZOIL-N-pyridyloxyphenylurea Surface-active substance Solvent
30-50
5-20 Else
Priority by featured. . Hydrogen is added, on the lesser - 07.09.79 at X, - hydrogen, chlorine,
at least one of X and X Vl-Fluorine, bromine, methyl, nitro group; X is methyl, ethyl hydrogen, chlorine, fluorine; X and X - water propyl, methylcarbonyl-genus, methyl, chlorine; X - hydrogen, chlorine,
howl, methoxycarbonylC, -C-alkyl; Xg is methyl, hydrogen,
or an ethoxycarbonyl group — chlorine; XY - hydrogen, chlorine, fluorine, sing, 08.02.80 with Hu - methylcarbonyl,
as surfactant ve-alkoxy C-C -carbonyl; X - methoxides - .polyoxyethylene styryl (alkyl) sigroup, nitro.
,Table 1
N-Benzoyl-T-pyridyloxyphenylurea
Derivative N-benz-ZOIL-N-pyridyloxy-siphenyl urea Surface-active substance Solvent
Continuation of table 1
g) -CONHCONH- / O) - O
FPI4.
Offered
C1
100 100 100 100 100 100
SNZ GVg
; O; -SOYNSOSCHO) -OCHO SGS10o yuo 90. 85 100 100 CF
F.
CONHCONH- / O) -0 fey-CF
F N CHZ
xF Cl
OyCONHCONR - (oV-0-4O -CF7ioo loo loo loo loo loo MpM Ъ1-
SNS
.F%
O -CONHCOfNH- / O)) - CF 5ioo loo loo loo lOo loo
(
,
FS, Cl
; oyc6NHcoNH4O -o- oV-cF3
M N- COOCH j
СНз Cl Р) -СОСОCO Н- ОХ- 0 nfeVcFT, 100 100
FM
SOOSNz
100 100 100 100 100 100
100 100 100 100100 100
100 100100100
(o) -СГз1оо
FM 1 COOC2H5
Br
Sb-CO HCOMH- / oV-0- CF4 N-
100
SOOSzNb
100 905050
100 10095 906050
Compounds
Compare Compounds
BUT
СХ1ЫНСОЪ1Н- (о) 0- / 5УВг2о
  lt tf
Xi
BS1
; OVC01 HCONH- §KO - (O) -Cl70 TC1
FВ
®soyonsomnoo-o) -o- / o) -sge
L
Cl
Editor O. Bugir
Compiled by N.Golubeva Tekhred L. Serdyukova
Order 2881/58 Circulation 629Subscription
VNIIPI USSR State Committee
for inventions and discoveries 113035, Moscow, Zh-35, Raushsk nab ,, d.4 / 5
 arj i M-- | n -M - L.tf -raj- -Gsh-H-Ya-- | -t-1-MPg-Jt Tr --- --- -Production and Printing Enterprise, Uzhgorod, ul. Project, 4
oh oh
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ABOUT
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Proofreader L. Patay

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引用文献:

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公开号 | 申请日 | 公开日 | 申请人 | 专利标题

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NL160809C|1970-05-15|1979-12-17|Duphar Int Res|METHOD FOR PREPARING BENZOYLURUM COMPOUNDS, AND METHOD FOR PREPARING INSECTICIDE PREPARATIONS BASED ON BENZOYLURUM COMPOUNDS.|

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US3931201A|1974-01-22|1976-01-06|The Dow Chemical Company|Substituted pyridinyloxyphenyl -acetamides, -ureas and urea derivatives|

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US4173637A|1976-10-29|1979-11-06|Ishihara Sangyo Kaisha Ltd.|N-Benzoyl-N'-pyridyloxy phenyl urea and insecticidal compositions thereof|

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JPS5840946B2|1976-10-29|1983-09-08|Ishihara Mining & Chemical Co|

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JPS5823871B2|1978-02-06|1983-05-18|Ishihara Mining & Chemical Co|DE3275720D1|1981-11-10|1987-04-23|Ciba Geigy Ag|PHENYLBENZOYL UREAS AS PESTICIDES|

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US5416102A|1981-11-10|1995-05-16|Ciba-Geigy Corporation|Method of preventing the reinfestation of dogs and cats by fleas|

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JPS6193163A|1984-10-12|1986-05-12|Ishihara Sangyo Kaisha Ltd|N-benzoyl-n'-phenylurea compound, its preparation and carcinostatic agent containing same|

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US5135953A|1984-12-28|1992-08-04|Ciba-Geigy|Use of acyl urea compounds for controlling endoparasites and ectoparasites of warm-blooded animals|

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DE3545569A1|1985-12-21|1987-06-25|Hoechst Ag|NEW PYRIDINE DERIVATIVES, METHOD FOR THE PRODUCTION THEREOF, CONTAINERS THEREOF AND THEIR USE AS A PEST CONTROL|

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NZ221964A|1986-10-03|1990-03-27|Ishihara Sangyo Kaisha|Benzoylurea compounds and insecticidal compositions|

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EP0360748A1|1988-09-21|1990-03-28|Ciba-Geigy Ag|Benzoylphenylureas|

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法律状态:

优先权:

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申请号 | 申请日 | 专利标题

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JP11486279A|JPS6317062B2|1979-09-07|1979-09-07|

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JP1443080A|JPS6317063B2|1980-02-08|1980-02-08|

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